The Resource Practical instrumental analysis : methods, quality assurance and laboratory management, Sergio Petrozzi, (electronic resource)

Practical instrumental analysis : methods, quality assurance and laboratory management, Sergio Petrozzi, (electronic resource)

Label
Practical instrumental analysis : methods, quality assurance and laboratory management
Title
Practical instrumental analysis
Title remainder
methods, quality assurance and laboratory management
Statement of responsibility
Sergio Petrozzi
Creator
Subject
Genre
Language
  • eng
  • eng
Summary
This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation.What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be ""fit for purpose"".The book presents sixteen experiments
Cataloging source
MiAaPQ
http://library.link/vocab/creatorName
Petrozzi, Sergio
Dewey number
543
Index
index present
Language note
English
LC call number
QD79.I5
LC item number
P48 2012
Literary form
non fiction
Nature of contents
  • dictionaries
  • bibliography
http://library.link/vocab/subjectName
  • Instrumental analysis
  • Chemistry, Analytic
Label
Practical instrumental analysis : methods, quality assurance and laboratory management, Sergio Petrozzi, (electronic resource)
Instantiates
Publication
Note
Description based upon print version of record
Bibliography note
Includes bibliographical references and index
Carrier category
online resource
Carrier category code
  • cr
Content category
text
Content type code
  • txt
Contents
  • Title page; Copyright page; Contents; Preface to the German Edition; Preface to the English Edition; Dedication; Foreword; 1: Introduction; 1.1 Analytical Chemistry - The History; 1.2 Analytical Chemistry and Its Role in Today's Society; 2: Introduction to Quality Management; 2.1 Historical Background; 2.2 Variability; 2.3 The Four Pillars of Wisdom (from Shewhart to Deming); 2.4 Zero-Defect Tolerance; 2.5 Why Standards?; 2.6 The Controlled Process; 2.7 ISO Guidelines 9004; 2.8 Quality Management System (QMS) Requirements; 3: Fundamentals of Statistics; 3.1 Basic Concepts
  • 3.1.1 Population and Sample3.1.2 Distribution of Values; 3.2 Important Terms; 3.2.1 Mean, Arithmetic Mean, Average (); 3.2.2 Standard Deviation (σ, s); 3.2.3 Variance (Var,V); 3.2.4 Standard Deviation of Mean Values (); 3.2.5 Relative Standard Deviation (RSD) and Coefficient of Variation (CV); 3.2.6 Confidence Interval (CI), Confidence Limits; 3.3 Quality of Results (Accuracy and Precision); 3.3.1 Measurement Deviations; 3.3.2 Random Deviations - Influence on Precision; 3.3.3 Systematic Deviations - Influence on Accuracy; 3.3.4 Gross Errors; 3.3.5 Uncertainty of Measurement Results
  • 3.3.6 Non-statistical Methods of Estimation3.3.7 Expressing Analytical Results; 3.3.8 Significant Figures - "Box-and-Dot" Method; 3.3.9 Outlier Tests; 3.4 Regression; 3.4.1 Regression Analysis; 3.4.2 Calibration Function; 3.4.3 The "Optimal" Trend Line; 3.4.4 Linear Regression; 4: The Analytical Process; 4.1 The Analytical Process in the Overall Context; 4.2 Planning Phase; 4.2.1 Analytical Problem; 4.2.2 Object of Investigation; 4.2.3 Sample; 4.2.4 Sampling; 4.2.5 Examination Procedures; 4.2.6 Analyte; 4.2.7 Literature and Database Research; 4.3 Analysis; 4.3.1 Measurement
  • 4.3.2 Method Optimization4.3.3 Calibration; 4.4 Assessment; 4.4.1 Quantification; 4.4.2 ("True") Content; 4.5 Validation; 4.5.1 Validation Elements; 4.5.2 Using the Computer; 4.6 Final Documentation; 4.6.1 Review; 5: Example of a Validation Strategy; 5.1 Determination of Phenol in Industrial Waste Water; 5.1.1 Confirmation of Identity; 5.1.2 Sample Content Determination; 5.1.3 Selection; 6: Organizational and Practical Procedures in the Teaching Laboratory Program; 6.1 Goals; 6.2 Safety in the Laboratory Class; 6.3 Experimental Project Workflow; 6.3.1 Preparation; 6.3.2 Laboratory Notebook
  • 6.4 ReportsReferences; 7: Literature; 7.1 Cited Literature; 7.2 Recommended Norms (Selection); 7.2.1Calibration; 7.2.2Inter-laboratory Tests; 7.2.3Quality Management; 7.3 Suggested Books (Selection); 8: Projects; 8.1 Chromatography; 8.1.1 Gas Chromatography - GC, Project: Tanker Accident; 8.1.1.1 Analytical Problem; 8.1.1.2 Introduction; 8.1.1.3 Material and Methods; 8.1.1.4 Questions; References; 8.1.2 Gas Chromatography Coupled with Mass Selective Detection - GC/MS, Project: "Circumvention of the Formerly Mandatory Declaration of Fragrances in Perfumes?"; 8.1.2.1 Analytical Problem
  • 8.1.2.2 Introduction
Dimensions
unknown
Extent
1 online resource (493 p.)
Form of item
online
Isbn
9783527665914
Media category
computer
Media type code
  • c
Specific material designation
remote
System control number
  • (CKB)2670000000263092
  • (EBL)1037094
  • (OCoLC)817822759
  • (SSID)ssj0000773050
  • (PQKBManifestationID)11493637
  • (PQKBTitleCode)TC0000773050
  • (PQKBWorkID)10826226
  • (PQKB)11258729
  • (MiAaPQ)EBC1037094
  • (EXLCZ)992670000000263092
Label
Practical instrumental analysis : methods, quality assurance and laboratory management, Sergio Petrozzi, (electronic resource)
Publication
Note
Description based upon print version of record
Bibliography note
Includes bibliographical references and index
Carrier category
online resource
Carrier category code
  • cr
Content category
text
Content type code
  • txt
Contents
  • Title page; Copyright page; Contents; Preface to the German Edition; Preface to the English Edition; Dedication; Foreword; 1: Introduction; 1.1 Analytical Chemistry - The History; 1.2 Analytical Chemistry and Its Role in Today's Society; 2: Introduction to Quality Management; 2.1 Historical Background; 2.2 Variability; 2.3 The Four Pillars of Wisdom (from Shewhart to Deming); 2.4 Zero-Defect Tolerance; 2.5 Why Standards?; 2.6 The Controlled Process; 2.7 ISO Guidelines 9004; 2.8 Quality Management System (QMS) Requirements; 3: Fundamentals of Statistics; 3.1 Basic Concepts
  • 3.1.1 Population and Sample3.1.2 Distribution of Values; 3.2 Important Terms; 3.2.1 Mean, Arithmetic Mean, Average (); 3.2.2 Standard Deviation (σ, s); 3.2.3 Variance (Var,V); 3.2.4 Standard Deviation of Mean Values (); 3.2.5 Relative Standard Deviation (RSD) and Coefficient of Variation (CV); 3.2.6 Confidence Interval (CI), Confidence Limits; 3.3 Quality of Results (Accuracy and Precision); 3.3.1 Measurement Deviations; 3.3.2 Random Deviations - Influence on Precision; 3.3.3 Systematic Deviations - Influence on Accuracy; 3.3.4 Gross Errors; 3.3.5 Uncertainty of Measurement Results
  • 3.3.6 Non-statistical Methods of Estimation3.3.7 Expressing Analytical Results; 3.3.8 Significant Figures - "Box-and-Dot" Method; 3.3.9 Outlier Tests; 3.4 Regression; 3.4.1 Regression Analysis; 3.4.2 Calibration Function; 3.4.3 The "Optimal" Trend Line; 3.4.4 Linear Regression; 4: The Analytical Process; 4.1 The Analytical Process in the Overall Context; 4.2 Planning Phase; 4.2.1 Analytical Problem; 4.2.2 Object of Investigation; 4.2.3 Sample; 4.2.4 Sampling; 4.2.5 Examination Procedures; 4.2.6 Analyte; 4.2.7 Literature and Database Research; 4.3 Analysis; 4.3.1 Measurement
  • 4.3.2 Method Optimization4.3.3 Calibration; 4.4 Assessment; 4.4.1 Quantification; 4.4.2 ("True") Content; 4.5 Validation; 4.5.1 Validation Elements; 4.5.2 Using the Computer; 4.6 Final Documentation; 4.6.1 Review; 5: Example of a Validation Strategy; 5.1 Determination of Phenol in Industrial Waste Water; 5.1.1 Confirmation of Identity; 5.1.2 Sample Content Determination; 5.1.3 Selection; 6: Organizational and Practical Procedures in the Teaching Laboratory Program; 6.1 Goals; 6.2 Safety in the Laboratory Class; 6.3 Experimental Project Workflow; 6.3.1 Preparation; 6.3.2 Laboratory Notebook
  • 6.4 ReportsReferences; 7: Literature; 7.1 Cited Literature; 7.2 Recommended Norms (Selection); 7.2.1Calibration; 7.2.2Inter-laboratory Tests; 7.2.3Quality Management; 7.3 Suggested Books (Selection); 8: Projects; 8.1 Chromatography; 8.1.1 Gas Chromatography - GC, Project: Tanker Accident; 8.1.1.1 Analytical Problem; 8.1.1.2 Introduction; 8.1.1.3 Material and Methods; 8.1.1.4 Questions; References; 8.1.2 Gas Chromatography Coupled with Mass Selective Detection - GC/MS, Project: "Circumvention of the Formerly Mandatory Declaration of Fragrances in Perfumes?"; 8.1.2.1 Analytical Problem
  • 8.1.2.2 Introduction
Dimensions
unknown
Extent
1 online resource (493 p.)
Form of item
online
Isbn
9783527665914
Media category
computer
Media type code
  • c
Specific material designation
remote
System control number
  • (CKB)2670000000263092
  • (EBL)1037094
  • (OCoLC)817822759
  • (SSID)ssj0000773050
  • (PQKBManifestationID)11493637
  • (PQKBTitleCode)TC0000773050
  • (PQKBWorkID)10826226
  • (PQKB)11258729
  • (MiAaPQ)EBC1037094
  • (EXLCZ)992670000000263092

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